Experiment OP - unpublished/hörstelCL/3
| Article DOI | N/A | ||||||
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| Data DOI | 10.57992/nmrxiv.p157.s1604 | ||||||
| Internal ID | unpublished/hörstelCL/3 | ||||||
| Membrane composition (molar fraction) |
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| Solution composition |
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| Temperature (K) | 300.5 | ||||||
| Total hydration | 30 (mass %) | ||||||
| pH | UNKNOWN | ||||||
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| Sample protocol | TLCL_0H/Na+ (27.3mg, 1.0 eq.) and DSS (0.25mg, 0.06eq.) were dissolved with 1ml chloroform:methanol (7:3, v/v) in an Eppendorf vial. The solvent was evaporated at 40°C under a constant stream of argon and freeze-dried over night. 18.0µl degassed water was added and the Eppendorf was stored at 40°C for three days. Lost water was added and the sample was mixed thoroughly with a steel rod. After another two days of equilibration the sample was again mixed before packing the insert. Hydration by 1H MAS NMR: 18 per phosphate, Na+ concentration guessed | ||||||
| Show on GitHub | experiments/OrderParameters/unpublished/hörstelCL/3 main |
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| ADDITIONAL_MOLECULES |
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| NMR |
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